Annual Reports on NMR Spectroscopy Volume 62 1st Edition by Graham Webb 9780123739193 0123739195
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Product details:
ISBN 10: 0123739195
ISBN 13: 9780123739193
Author: Graham A. Webb
Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has grown to such importance as NMR spectroscopy. It is used in all branches of science when precise structural determination is required and when the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and nonspecialist alike to become familiar with new techniques and applications of NMR spectroscopy.
* Provides updates on the latest developments in NMR spectroscopy
* Includes comprehensive review articles
* Highlights the increasing importance of NMR spectroscopy as a technique for structural determination
Table of contents:
Chapter 1. Flow techniques in NMR spectroscopy
1. Introduction
2. The Start of Flow NMR and the Evolution of LC-NMR
3. Non-Chromatographic Flow NMR
4. New Technologies to Facilitate Flow NMR
5. Variations of the Flow Techniques/Fluidics
6. Applications
7. Problems and Challenges
8. Conclusions
Acknowledgments
References
Chapter 2. Vanadium-51 NMR
1. Introduction
2. Isotropic Systems
3. Solid-State Parameters
4. Mesophases
5. Computational Methods
6. Concluding Remarks
Acknowledgments
References
Chapter 3. Solid-State Effects on NMR Chemical Shifts
1. Introduction
2. Origin of Solid-State Effects on Chemical Shifts
3. Theoretical Methods
4. Case Studies of Solid-State Effects
5. Concluding Remarks
Acknowledgments
References
Chapter 4. NMR Studies of Encapsulated Macromolecules
1. Introduction
2. The Challenge of Complex Biomacromolecules
3. The Rate of NMR Relaxation Depends on the Molecular Tumbling Rate
4. Reverse Micelles
5. Water in Reverse Micelles
6. Thermodynamics of Reverse Micelle Particle Formation
7. Proteins Encapsulated by Reverse Micelles
8. Encapsulation Protocols
9. Solvent Suppression
10. Hydrodynamic Behavior of AOT Reverse Micelle Assemblies
11. Practical Application of Reverse Micelle Encapsulation to Larger Polypeptides
12. Multinuclear Resonance Assignments of Encapsulated Proteins
13. Structural Studies of Encapsulated Macromolecules
14. Low Temperature NMR Studies of Encapsulated Water
15. Thermodynamics of Water Shedding – A Concise Analysis
16. Low Temperature Studies of Encapsulated Proteins
17. Effect of Reverse Micelle Encapsulation on Motional Dynamics in Polypeptides
18. Future Studies
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