Nanoscale Ferroelectrics and Multiferroics Key Processing and Characterization Issues and Nanoscale Effects 1st Edition by Miguel Alguero, J Marty Gregg, Liliana Mitoseriu ISBN 1118935756 9781118935750

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ISBN 10: 1118935756 
ISBN 13: 9781118935750
Author: Miguel Alguero, J Marty Gregg, Liliana Mitoseriu

This two volume set reviews the key issues in processing and characterization of nanoscale ferroelectrics and multiferroics, and provides a comprehensive description of their properties, with an emphasis in differentiating size effects of extrinsic ones like boundary or interface effects. Recently described nanoscale novel phenomena are also addressed. Organized into three parts it addresses key issues in processing (nanostructuring), characterization (of the nanostructured materials) and nanoscale effects. Taking full advantage of the synergies between nanoscale ferroelectrics and multiferroics, the text covers materials nanostructured at all levels, from ceramic technologies like ferroelectric nanopowders, bulk nanostructured ceramics and thick films, and magnetoelectric nanocomposites, to thin films, either polycrystalline layer heterostructures or epitaxial  systems, and to nanoscale free standing objects with specific geometries, such as nanowires and tubes at different levels of development. This set is developed from the high level European scientific knowledge platform built within the COST (European Cooperation in Science and Technology) Action on Single and multiphase ferroics and multiferroics with restricted geometries (SIMUFER, ref. MP0904). Chapter contributors have been carefully selected, and have all made major contributions to knowledge of the respective topics, and overall, they are among most respected scientists in the field.

Nanoscale Ferroelectrics and Multiferroics Key Processing and Characterization Issues and Nanoscale Effects 1st Table of contents:

PART A Nanostructuring: Bulk
1 Incorporation Mechanism and Functional Properties of Ce-Doped BaTiO3 Ceramics Derived from Nanopowders Prepared by the Modified Pechini Method
1.1 Why Cerium-Doped BaTiO3?
1.2 Sample Preparation, Phase and Nano/Microstructural Characterization
1.3 Dielectric Properties
1.4 Raman Investigation
1.5 Conclusions
Acknowledgments
References
2 Synthesis and Ceramic Nanostructuring of Ferroic and Multiferroic Low-Tolerance-Factor Perovskite Oxides
2.1 Introduction
2.2 Synthesis of Perovskites Oxides
2.3 Processing of Ferroic and Multiferroic Materials:honey From the Ceramic Method to the Current Assisted Methods
2.4 Combination of Mechanosynthesis and Spark Plasma Synthesis:honey The Right Track to the Nanoscale in Ferroic Materials
2.5 Conclusions
Acknowledgments
References
3 Core–Shell Heterostructures:honey From Particle Synthesis to Bulk Dielectric, Ferroelectric, and Multiferroic Composite Materials
3.1 Introduction
3.2 Liquid-Phase Synthesis of Core–Shell Particles
3.3 BaTiO3@polymer Particles and Composites
3.4 Inorganic Core–Shell Particles with a Ferroelectric Core
3.5 Multiferroic Core–Shell Particles and Composites
3.6 Conclusions and Outlook
References
4 Modeling of Colloidal Suspensions for the Synthesis of the Ferroelectric Oxides with Complex Chemical Composition
4.1 Introduction
4.2 Solid-State Synthesis
4.3 Colloidal Interactions and Aggregation
4.4 Aggregation in the Three-Component System
4.5 Applying the Modeling Results to Enhance Properties of Ferroelectric Complex Oxides
4.6 Conclusions and Outlook
Acknowledgments
References
5 Self-Assemblage and Patterning of Thin-Film Ferroic Nanostructures
5.1 Introduction
5.2 Short Survey on Classical Top-Down Approaches
5.3 Non-invasive Procedures
5.4 Embedded Ferroelectric Nanograins
5.5 Conclusions
References
6 Thin-Film Porous Ferroic Nanostructures:honey Strategies and Characterization
6.1 (Nano)Microelectronics Considerations
6.2 Ferroics and Nanoferroic Structures
6.3 Meso- and Nanoporosity in Advanced Functional Materials
6.4 Nanoporosity in Ferroelectric Thin Films
6.5 Looking Ahead
Acknowledgments
References
7 Low-Temperature Photochemical Solution Deposition of Ferroelectric and Multiferroic Thin Films
7.1 Introduction
7.2 Low-Temperature Processing of Ferroelectrics and Multiferroics
7.3 Low Environmental Impact Precursor Chemistry
7.4 Aquous Solution–Gel Precursors
7.5 Photosensitive Sol–Gel Precursors
7.6 Photochemical Solution Deposition (PCSD)
7.7 Final Remarks
References
8 Synthesis and Properties of Ferroelectric Nanotubes and Nanowires:honey A Review
8.1 Introduction
8.2 Synthesis of Ferroelectric Nanowires and Nanotubes
8.3 Crystal Structure, Phase Transitions, and Ferroelectric Properties
8.4 Applications
8.5 Summary and Conclusions
References
9 Fabrication of One-Dimensional Ferroelectric Nano- and Microstructures by Different Spinning Techniques and Their Characterization
9.1 Introduction
9.2 Fiber Synthesis
9.3 Investigation of Nanostructure, Microstructure, and Phase Composition
9.4 Investigation of Mechanical Properties
9.5 Ferroelectric Characterization
9.6 Applications
9.7 Summary and Outlook
References
PART B: Characterization (of the Nanostructured Materials): Crystal Structure
10 Structural Characterization of Ferroelectric and Multiferroic Nanostructures by Advanced TEM Techniques
10.1 Introduction:honey Advanced TEM Techniques for the Analysis of Ferroelectric and Multiferroic Materials
10.2 Transmission Electron Microscopy
10.3 HAADF–STEM Structure Determination
10.4 Electron Energy Loss Spectroscopy
10.5 Future and Challenges
References
11 Raman Spectroscopy of Nanostructured Ferroelectric Materials
11.1 Introduction
11.2 Raman Spectroscopy Fundamentals
11.3 Raman Analysis of Relaxors
11.4 Raman Analysis of Nanostructured Ferroelectrics
11.5 Tip-Enhanced Raman Spectroscopy (TERS) of Nanoscale Ferroelectrics
11.6 Summary
Acknowledgments
References
12 Neutron and Synchrotron X-Ray Scattering Studies of Bulk and Nanostructured Multiferroic and Ferroelectric Materials
12.1 Introduction
12.2 Synchrotron X-Ray and Neutron Facilities for Structural Characterization of Ferroelectrics and Multiferroics
12.3 Crystal Structure of NdMn2O5 in Powder and Single Crystalline Forms
12.4 Neutron Total Scattering Investigations of the BaTiO3@SiO2 Nanocomposites
12.5 Concluding Comments
Acknowledgments
References
13 Advanced Characterization of Multiferroic Materials by Scanning Probe Methods and Scanning Electron Microscopy
13.1 SPM-Related Methods in Advanced Materials Research
13.2 Magnetic Force Microscopy (MFM) and Related Methods
13.3 Electrostatic Force Microscopy (EFM) and Piezo Force Microscopy (PFM)
13.4 Scanning Tunneling Microscopy (STM) and Related Methods
13.5 Imaging of Crystallographic Orientations (SEM/EBSD)
13.6 New Developments in the Field of EBSD
References
14 Electrostatic and Kelvin Probe Force Microscopy for Domain Imaging of Ferroic Systems
14.1 Introduction
14.2 Electrostatic Force Microscopy and Kelvin Probe Force Microscopy
14.3 EFM of Ferroelectric Materials
14.4 KPFM of Ferroelectric Materials
14.5 Recent Advances
14.6 Summary and Outlook
Acknowledgments
References
VOLUME II
PART C: Nanoscale Effects: Bulk Properties
15 Nanostructured Barium Titanate Ceramics:honey Intrinsic versus Extrinsic Size Effects
15.1 Introduction
15.2 Applications of BaTiO3 Ceramics; Actual Demands for Passive Components
15.3 Size-Dependent Phenomena in Ferroelectrics
15.4 Size-Dependent Properties in BaTiO3 Ceramics:honey Intrinsic versus Extrinsic Size Effects
15.5 Conclusions
Acknowledgments
References
16 The Effects of Ceramic Nanostructuring in High-Sensitivity Piezoelectrics
16.1 Technological Drive for Ceramic Nanostructuring of High-Sensitivity Piezoelectrics
16.2 State of the Art Ferroelectric Materials for Piezoelectric Technologies
16.3 Nanostructuring Effects in Perovskite Systems with PZT-like MPBs
16.4 Nanostructuring Effects in Perovskite Systems with Intrinsic Chemical Inhomogeneity
16.5 Summary and Future Perspectives
16.6 Acknowledgments
References
17 Correlation between Microstructure and Electrical Properties of Ferroelectric Relaxors
17.1 Introduction
17.2 Perovskite Relaxors
17.3 Aurivillius Lead-Free Ferroelectric Relaxors
17.4 Conclusions
References
18 Local Field Engineering Approach for Tuning Dielectric and Ferroelectric Properties in Nanostructured Ferroelectrics and Composites
18.1 Introduction
18.2 Finite Element Method
18.3 The Role of Local Electric Field Inhomogeneity on Tunability Properties
18.4 Switching Properties in Inhomogeneous Ferroelectrics
18.5 Conclusions
18.6 Acknowledgments
References
19 Ferroelectric Phase Transitions in Epitaxial Perovskite Films
19.1 Introduction
19.2 Experimental Study of Phase Transition
19.3 Dielectric Permittivity in Thin Films
19.4 Phase Transitions in Epitaxial Films
19.5 Concluding Remarks
19.6 Acknowledgments
References
20 Interfaces in Epitaxial Ferroelectric Layers/Multilayers and Their Effect on the Macroscopic Electrical Properties
20.1 Introduction
20.2 Electrode Interfaces in Ferroelectric Capacitors
20.3 Interfaces in Complex Structures
20.4 Conclusions
Acknowledgments
References
21 Electric Field Control of Magnetism Based on Elastically Coupled Ferromagnetic and Ferroelectric Domains
21.1 Introduction
21.2 Domain Pattern Transfer
21.3 Elastic Coupling Between Magnetic and Ferroelectric Domain Walls
21.4 Domain Size Scaling of Pattern Transfer
21.5 Electric Field Control of Ferromagnetic Domains
21.6 Electric Field Driven Magnetic Domain Wall Motion
21.7 Summary and Outlook
Acknowledgments
References
22 Ferroelectric Vortices and Related Configurations
22.1 Insights from Simulations and Theory
22.2 Insights from Experiments
Acknowledgments
References
23 Reentrant Phenomena in Relaxors
23.1 Introduction
23.2 Reentrant Phases in Condensed Matter
23.3 Relaxor Ferroelectrics
23.4 Reentrant Relaxor Behavior in Ferroelectrics
23.5 Transverse Glassy Freezing and Canonical Relaxors
23.6 Reentrant Dipolar Glass State in Quantum Paraelectrics Doped with Dipolar Impurities
23.7 Summary and Concluding Remarks
Acknowledgments
References
24 Functional Twin Boundaries:honey Multiferroicity in Confined Spaces
24.1 Introduction
24.2 Ferroelectric Twin Boundaries
24.3 Conducting Twin Boundaries
24.4 Thermal Conductivity
24.5 Landau Theory of Coupled Order Parameters in Domain Walls
24.6 Chiral Twin Walls
24.7 High Wall Densities
24.8 Summary
Acknowledgment
References
25 Novel Approaches for Genuine Single-Phase Room Temperature Magnetoelectric Multiferroics
25.1 Introduction to Single-Phase Multiferroic Materials
25.2 Aurivillius Phase Materials – Candidate Single-Phase Multiferroics?
25.3 Magnetoelectric Coupling in Multiferroic Bi6TixFeyMnzO18 Systems at Room Temperature
25.4 Confidence Level Assessment of Genuine Single-Phase Multiferroicity
25.5 Potential Devices/Applications Based on Single-Phase Magnetoelectric Multiferroics
25.6 Summary and Conclusions
References
26 Semiconducting and Photovoltaic Ferroelectrics
26.1 Introduction
26.2 Basic Principles of Photovoltaic Effect in Ferroelectrics
26.3 Experimental Evidence of the Bulk Photovoltaic Effect in Ferroelectrics
26.4 The Role of the Schottky Barrier and Depletion Layer
26.5 Photovoltaic Effect Mediated by Ferroelectric Domain Walls
26.6 Ferroelectric Solid Solutions:honey Chemical Tuning of Band-Gap
26.7 Conclusions

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Tags: Miguel Alguero, J Marty Gregg, Liliana Mitoseriu, Nanoscale, Ferroelectrics