Purification of Laboratory Chemicals 5th Edition by Wilfred Armarego, Christina Li Lin Chai 0750675713 9780750675710

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ISBN 10: 0750675713

ISBN 13: 9780750675710

Author: Wilfred L.F. Armarego and Christina Li Lin Chai

Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.

In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.

* Complete update of this valuable, well-known reference
* Provides purification procedures of commercially available chemicals and biochemicals
* Includes an extremely useful compilation of ionisation constants

Purification of Laboratory Chemicals 5th Table of contents:

CHAPTER 1. COMMON PHYSICAL TECHNIQUES USED IN PURIFICATION
INTRODUCTION
THE QUESTION OF PURITY
SOURCES OF IMPURITIES
PRACTICES TO AVOID IMPURITIES
SAFETY PRECAUTIONS ASSOCIATED WITH THE PURIFICATION OF LABORATORY CHEMICALS
SOME HAZARDS OF CHEMICAL MANIPULATION IN PURIFICATION AND RECOVERY OF RESIDUES
SAFETY DISCLAIMER
METHODS OF PURIFICATION OF REAGENTS AND SOLVENTS
SOLVENT EXTRACTION AND DISTRIBUTION
DISTILLATION
RECRYSTALLISATION
SUBLIMATION
CHROMATOGRAPHY
DRYING
MISCELLANEOUS TECHNIQUES
ABBREVIATIONS
TABLES
BIBLIOGRAPHY

CHAPTER 2. CHEMICAL METHODS USED IN PURIFICATION
GENERAL REMARKS
REMOVAL OF TRACES OF METALS FROM REAGENTS
METAL IMPURITIES
DISTILLATION
USE OF ION EXCHANGE RESINS
PRECIPITATION
EXTRACTION
COMPLEXATION
USE OF METAL HYDRIDES
LITHIUM ALUMINIUM HYDRIDE
CALCIUM HYDRIDE
SODIUM BOROHYDRIDE
POTASSIUM BOROHYDRIDE
PURIFICATION via DERIVATIVES
ALCOHOLS
ALDEHYDES
AMINES
AROMATIC HYDROCARBONS
CARBOXYLIC ACIDS
HYDROPEROXIDES
KETONES
PHENOLS
PHOSPHATE AND PHOSPHONATE ESTERS
MISCELLANEOUS
GENERAL METHODS FOR THE PURIFICATION OF CLASSES OF COMPOUNDS PROCEDURES
CRITERIA OF PURITY
GENERAL PROCEDURES FOR THE PURIFICATION OF SOME CLASSES OF ORGANIC COMPOUNDS
ACETALS
ACIDS
ACID CHLORIDES
ALCOHOLS
ALDEHYDES
AMIDES
AMINES
AMINO ACIDS
ANHYDRIDES
CAROTENOIDS
ESTERS
ETHERS
HALIDES
HYDROCARBONS
IMIDES
IMINO COMPOUNDS
KETONES
MACROMOLECULES
NITRILES
NITRO COMPOUNDS
NUCLEIC ACIDS
PHENOLS
POLYPEPTIDES AND PROTEINS
QUINONES
SALTS (ORGANIC)
SULFUR COMPOUNDS
BIBLIOGRAPHY

CHAPTER 3. THE FUTURE OF PURIFICATION
INTRODUCTION
SOLID PHASE SYNTHESIS
SOLID PHASE PEPTIDE SYNTHESIS (SPPS)
SOLID PHASE DEOXYRIBONUCLEOTIDE SYNTHESIS
SOLID PHASE OLIGOSACCHARIDE SYNTHESIS
SOLID PHASE ORGANIC SYNTHESIS (SPOS)
POLYMER SUPPORTED REACTANTS
SCAVENGER RESINS
RESIN SUPPORT
CHOICE OF RESIN FOR SPOS
COMBINATORIAL CHEMISTRY
MONITORING SOLID PHASE REACTIONS
DETECTION OF REACTIVE GROUPS ON RESINS
IONIC LIQUIDS
FLUOROUS CHEMISTRY
BIBLIOGRAPHY

CHAPTER 4. PURIFICATION OF ORGANIC CHEMICALS

CHAPTER 5. PURIFICATION OF INORGANIC AND METALORGANIC CHEMICALS (Including Organic compounds of B, B

CHAPTER 6. PURIFICATION OF BIOCHEMICALS AND RELATED PRODUCTS

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